D. Rohrbaugh, S. Munavalli, G. Wagner
Jan 1, 2001
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Phosphorus, Sulfur, and Silicon and the Related Elements
Abstract
Abstract Microwave catalyzed reaction of N-(2,3-epoxypropyl)phthalimide with H-dimethylphosphonate for 4 min yielded via free radical processes: trimethylphosphonate, trimethylphosphate, N-(2-propenyl)phthalimide, 2-(N-phthalimidopropyl) dimethylphosphinates, hydrogen 3-(N-phthalimidopropyl) methylphosphine oxide, hydrogen 3-(N-phthalimidopropyl)methylphosphinate, 2-(N-phthalimidopropyl) dimethylphosphonate, and 2-(N-phthalimidopropyl) dimethyl-phosph-inate. The mechanism of formation of the various compounds along with their mass spectral fragmentation behavior is described in this communication.