Feng Li
2012
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Journal
Journal of Synthetic Crystals
Abstract
The title complex,3,5-diiodosalicylaldehyde-phenylamine-zinc(Ⅱ) has been designed and microwave solid phase synthesized by 3,5-diiodosalicylaldehyde-phenylamine and zinc acetate.The structure was determined by IR spectra,elemental analysis and single X-ray crystallography.The title complex crystallizes in the monoclinic space group C2/c.Cell parameters: a=2.2287(2) nm,b=1.1699(4) nm,c=2.6065(3) nm,β=94.579(3)°,V=6.5667(12) nm3,Z=8,F(000)=3872,R[I2σ(I)],R1=0.0547,wR2=0.1316,S=1.024 The Zn(II) adopts a distorted tetrahedral geometry,coordinated by two nitrogens and two oxygens from 3,5-diiodosalicylaldehyde-phenylamine.