Li Jin-jin
2009
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Journal
Journal of Changsha University of Science & Technology
Abstract
2-(Benzo[d]thiazol-2-yl)isoindoline-1,3-dione was prepared with traditional and microwave technology,respectively.With microwave technology,the optimal parameters of microwave power,reactive time and ratio of reaction material were obtained as follows: microwave power 500 W,molar ratio of reaction material 1∶1.2,reaction time 6 min,product yield 90.8% in N,N-dimethylformamide solvent and product yield 87.4% in none solvent,respectively.