S. Hongbin
2011
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Journal
Modern Chemical Industry
Abstract
4,6-Dimethyl-2-(methylsulfonyl) pyrimidine was synthesized from acetylacetone by the cyclization,methylation and oxidation.The total yield was 61.23%.In the oxidation,oxone was first applied to the systhesis of 4,6-dimethyl-2-(methylsulfonyl) pyrimidine and its analogues,which made the oxidation to be safe and effective.The structure of target compound and its intermediates were confirmed by measurement of melting point,1HNMR,IR,MS.