D. Ismailova, R. Okmanov, A. Zi̇yaev
Feb 5, 2014
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Journal
Acta Crystallographica Section E: Structure Reports Online
Abstract
The title compound, C16H20N4OS2, was synthesized by the reaction of 2-benzylsulfanyl-5-chloroacetamido-1,3,4-thiadiazole and piperidine in a 1:2 ratio. The planes of the acetamide and 1,3,4-thiadiazole units are twisted by 10.8 (4)°. The thiadiazole S atom and the acetamide O atom are syn-oriented due to a hypervalent S⋯O interaction of 2.628 (4) Å. In the crystal, molecules form centrosymmetric dimers via N—H⋯N hydrogen bonds. These dimers are further connected by C—H⋯O interactions into (100) layers.