Guo Xiao-zhen
2011
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Journal
Journal of Jiangsu Teachers University of Technology
Abstract
2-Methylacetanilide was synthesized with O-toluidine as raw material and acetic acid as reagent of acylation.The factors that have influence on the action were investigated.The results showed that the optimal condition were molar ratio of Zinc of dosage with ratio of 2-toluidine to Zn 0.1mol:0.1g,the molar ratio of 2-toluidine to acetic acid 0.2:0.5;acylation 100~105℃,the yield of 2-Methylacetanilide such conditions was about 81.8%.