Li Jing-fen
2003
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Journal
Chinese Journal of Synthetic Chemistry
Abstract
2-Hydroxy-3-cyanmethylmethyl-5-methyl atophenone(5) was synthesized from p-methylphenol through acylating, Fries rearrangement reaction, chloromethylating and cyanating. The reactional conditions were optimized using the method of uniform experiment design to get 88.5% yield.