Huang Yu-ping
2007
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Journal
Chinese Journal of Medicinal Chemistry
Abstract
Fenticonazole nitrate was synthesized by phase-transfer catalysis from 1-(2,4-dichlorophenyl)-2-(N-imidazolyl)-ethanol and 1-chloromethyl-4-phenylthio-benzene.The target compound was identified by elemental analysis,IR,()1H-NMR and MS.The total yield is 56.5%.In comparison with the method reported,this method has several advantages of convenient operation,mild reaction conditions,cheap reagents and stable yield.This method is suitable for industrial process.