Kazuhito Hioki, K. Ohshima, Yuko Sota
Feb 1, 2009
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Journal
Synthesis
Abstract
A simple practical method for the synthesis of 4,6-aimetnoxy-1,3,5-triazin-2(1H)-one was developed. The desired product was easily obtained from 2-chloro-4,6-dimethoxy-1,3,5-triazine and acetic acid by shaking with dimethylamine-functionalized silica gel in ethanol. It was also demonstrated that the silica gel could be recycled by washing it with diluted aqueous ammonia solution.