Fang Hao
2010
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Journal
Chinese Journal of Pharmaceuticals
Abstract
1,2,3-Tri-O-acetyl-5-deoxy-D-ribofuranose was synthesized from D-ribose by methylation and protection with CuSO4/H2SO4/(CH3)2CO to give 1-O-methyl-2,3-O-isopropylidene-D-ribofuranose,which was subjected to esterification,reduction,deprotection and then acetylation with an overall yield of about 48%.