J. Hayes, H. Diehl, G. Smith
Jul 1, 1966
Citations
0
Influential Citations
0
Citations
Journal
Talanta
Abstract
Iodine is quantitatively oxidised to iodic acid by boiling with 70% perchloric acid and the iodic acid is isolated by cooling, filtering off the precipitated crystals, and washing them with concentrated nitric acid. The over-all stoichiometry of the reaction is one molecule of perchloric acid per atom of iodine.