B. Berrang, A. Lewin, F. Carroll
Nov 1, 2008
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Journal
Journal of Labelled Compounds and Radiopharmaceuticals
Abstract
Starting with [14C]-D-tyrosine, carbon-14 labeled JDTic dihydrochloride with specific activity 15 mCi/mol was prepared in 5% radiochemical yield. Separation of the (3R)- and (3S)-diastereomers was carried out via the 3-phenyl-2,3,10,10a-tetrahydro-5H-imidazo[1,5-b]isoquinolin-1-ones formed by reaction with benzaldehyde. Copyright © 2008 John Wiley & Sons, Ltd.