W. Nagata, M. Yoshioka, M. Murakami
Apr 28, 2003
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Journal
Organic Syntheses
Abstract
Preparation of cyano compounds using alkylaluminum intermediates: 1-cyano-6-methoxy-3,4-dihydronaphthalene reactant: 6.15 g. (0.0347 mole) of 6-methoxy-1-tetralone intermediate: p-toluenesulfonic acid monohydrate solvent: 1 l. of 40% ether in petroleum ether product: 1-cyano-6-methoxy-3,4-dihydronaphthalene Keywords: elimination, dehydration; apparatus, for transferring reaction mixture under inert atmosphere to acid quench; bubbler, mercury