P. Majewski
Sep 1, 1987
Citations
0
Influential Citations
3
Citations
Journal
Phosphorus Sulfur and Silicon and The Related Elements
Abstract
Abstract A novel convenient synthesis of dialkyl phosphorochloridites based on the reaction of trialkyl phosphites with dichlorotriphenylphosphorane has been described. In this way the commonly used dialkyl phosphorochloridites (3a–e) were prepared in satisfactory yields. Their identity was confirmed by 31P-NMR spectroscopy as well as by their refractive index.