Z. Yi
2010
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Journal
Journal of Shandong Institute of Light Industry
Abstract
Diethyl [[(p-Toluenesulfonyl)oxy]methyl] phosphonate was prepared from diethylphosphate,paraformal-dehyde and p-toluenesulfonic chloride by condensation and acylation.It was separated and purified by column chromatography.The amount of triethylamine and reaction time were examined.Product was characterized by IR and1HNMR,and the yield was 79.2%.