Ding Shao-min
2004
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Journal
Modern Chemical Industry
Abstract
A novel process to prepare highly pure 3-thiophenemethanol was provided.Thus,3-methylthiophene was chain-brominated and then directly hydrolyzed to produce crude 3-thiophenemethanol. After direct treatment with Zn/Cu powder under the alkaline condition and through simple distillation,3-thiophenemethanol was obtained to be 51.6% in over-all yield and 97. 8% purity,both exceed the traditional process.