Luo Yan-ping
2011
Citations
0
Influential Citations
2
Citations
Journal
Fine Chemical Intermediates
Abstract
2-Cyano-3-(2-nitrophenyl)-ethyl acrylate was converted to ethyl 2-aminoquinoline-3-carboxylate under reflux in acetic acid with iron powder as the reducing agent.The results showed that the optimum molar ratio of 2-cyano-3-(2-nitrophenyl)-ethyl acrylate to iron powder was 1 to 5,and the target compound was obtained in 94.7% yield with the structure confirmed by 1H NMR and GC-MS.