I. Yavari, H. Djahaniani
Sep 21, 2010
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Journal
Monatshefte für Chemie - Chemical Monthly
Abstract
Abstract2,6-Dimethylphenyl isocyanide reacts with benzoyl isothiocyanate in a clean one-pot reaction to afford a sterically congested ten-membered ring containing the S–S–S moiety in nearly quantitative yield. Dynamic effects are observed in the 1H nuclear magnetic resonance (NMR) spectrum of this compound for the restricted rotation around two of the Ar–N single bonds.Graphical abstract