Xiao Cui-ping
2009
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Journal
The Chemical Engineer
Abstract
Bis(2-chloroethyl)amine hydrochloride was synthesized from diethanol amine with thionyl chloride as chlorination agent and chloroform as solvent.The influence factors of usage of chloroform,the molar ratio of the materials,the reaction temperature and the reaction time were studied,and the optimal reaction conditions were obtained.The yield of bis(2-chloroethyl)amine hydrochloride was 84.6%.The result was identified by infrared spectrum.This process is simple,economic and environment-friendly.