A. Nikonov, I. Sterkhova, I. М. Lazarev
Oct 15, 2016
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Influential Citations
3
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Journal
Journal of Molecular Structure
Abstract
Abstract The N -(2-(trimethylsilyloxy)phenyl)acetamide 1 was synthesized via reaction of N -(2-hydroxyphenyl)acetamide with chlorotrimethylsilane. Transsilylation of new compound 1 by chloro(chloromethyl)dimethylsilane leads to 4-acetyl-2,2-dimethyl-3,4-dihydro-2H-1,4,2-benzoxazasiline 3 . The structures of the new compounds were investigated by 1 H, 13 C and 29 Si NMR spectroscopy, X-ray single-crystal analysis, FTIR spectroscopy and DFT methods.