H. Özay, M. Yıldız, H. Ünver
Jan 25, 2013
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Journal
Crystallography Reports
Abstract
The compound called 3-methoxy-2-[(2,4,4,6,6-pentachloro-1,3,5,2λ5,4λ5,6λ5-triazatriphosphin-2-yl)oxy]benzaldehyde has been synthesized from the reaction of 2-hydroxy-3-methoxybenzaldehyde with hexachlorocyclotriphosphazene. It has been characterized by elemental analysis, MS, IR, 1H NMR, 13C NMR, 31P NMR and UV-visible spectroscopic techniques. The structure of the title compound has been determind by X-ray analysis. Crystals are orthorhombic, space group P212121, Z = 4, a = 7.705(1), b = 12.624(1), c = 17.825(2) Å, R1 = 0.0390 and wR2 = 0.1074 [I > 2σ(I)], respectively.