U. Sarı, I. Yilmaz, K. Güven
Sep 1, 2004
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Journal
Journal of Chemical Crystallography
Abstract
Abstract2-{2-[3-Methyl-3-(2,4,6-trimethylphenyl)cyclobutyl]-2-oxoethyl}isoindole-1,3-dione (C24 H25NO3) was synthesized, and its crystal structure was determined by X-ray crystallographic techniques. The compound crystallizes in the triclinic space group P-1, with unit cell parameters: a = 14.109(9) Å, b = 14.130(8) Å, c = 12.152(6) Å, α = 105.62(5)°, β = 113.75(4)°, γ = 98.78(5)°, V = 2039.8(19) Å3, Dc= 1.223 g/cm3, and Z = 4. The crystal structure has two crystallographically independent molecules, I and II. These molecules are held together by weak intermolecular C—H···O interactions, forming a continuous chain. The dihedral angles between the N-substituted phthalimide moiety and cyclobutane ring in molecules I and II are 60.37(14) and 68.18(18)°, respectively.