N. Bayrak, M. Yıldız, H. Yıldırım
Nov 26, 2018
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Journal
Bulletin of the Chemical Society of Ethiopia
Abstract
2-(3,5-Dimethoxyphenylamino)-3-chloronaphthalene-1,4-dione compound was prepared from the nucleophilic substitution reaction of 2,3-dichloro-1,4-naphthoquinone with 3,5-dimethoxyphenylamine at reflux temperature according to literature reported previously. Single-crystal X-ray diffraction analysis was carried out to confirm the structure of the title compound. The title compound, C 18 H 14 ClNO 4 , crystallizes in the triclinic space group P-1, a = 7.0016(6) A, b = 7.7937(6) A, c = 15.6218(11) A, β = 97.238(4)°, V = 782.44(11) A 3 , Z = 2, R 1 = 0.0525, wR 2 = 0.1329. KEY WORDS : Naphthoquinones, Aminochloronaphthoquinone; X-Ray diffraction Bull. Chem. Soc. Ethiop. 2018 , 32(3), 603-608. DOI: https://dx.doi.org/10.4314/bcse.v32i3.18