Junzo Hirano, K. Hamase, T. Akita
2004
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Journal
Analytical Sciences: X-ray Structure Analysis Online
Abstract
The crystal structure of N-[(6-methoxy-4-oxo-1,4-dihydroquinolin-3-yl)methyl]-2,2-dimethylpropanamide (2) was determined by X-ray diffraction analysis. The compound crystallized in the triclinic system, space group P1, with cell parameters of a = 7.829(3)A, b = 8.995(4)A, c = 10.646(5)A, α = 85.86(2)°, β = 86.99(1)°, γ = 88.00(2)°, and Z = 2. The structure was refined by full-matrix least-squares to final values of R1 = 0.049 and wR2 = 0.103. The intermolecular hydrogen bonds of the type N-H…O were observed in the structure.