B. Hajjem, A. Kallel, I. Svoboda,
May 15, 1993
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Abstract
N-(4-Chloro-α,α-dimethoxybenzyl)acetamide, C 11 H 14 ClNO 3 , M r =243.69, orthorhombic, P2 1 2 1 2 1 , a=12.032 (4), b=10.724 (4), c=9.502 (3) A, V=1226 (1) A 3 , Z=4, D x =1.320 Mg m -3 , λ(Mo Kα)=0.71069 A, μ=0.301 mm -1 , F(000)=512, T=300 K, final R=0.043, wR=0.034 for 939 unique reflections with F >2σ(F). The conformation is characterized by an sp 3 -hybridized C atom which is connected to the N atom of the acetamide group