Li Xiu-lian
2009
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Journal
Chemical Reagents
Abstract
2,6-Difluorobenzamide was synthesized from 2,6-dichlorobenzonitrile via fluorination and hydrolysis with hydrogen peroxide.The overall product yield was 80.5% and its melting point was 145.4~145.6 ℃.The product structure was characterized by IR spectrometry and 1HNMR spectrometry.The production process features ready availability of starting materials,high product yield,good product quality,and less pollution to the environment.