Yang Hai-lang
2006
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Journal
Journal of Xiangfan University
Abstract
2-chloroethylamine hydrochloride was synthesized by the reaction of ethanolamine, dry hydrochloride with thionylchloride, chloroform as solvent. The optimum conditions was that: 1:1.04 molar ratio of ethanolamine to thionylchloride reacted at 71℃ for 24h after the ethanolamine had mixed with dry hydrochloride for In and chloroform as solvent. The yield was 98% with 99.9% purity.