Xu Shou-lin
2010
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Journal
Fine Chemical Intermediates
Abstract
3-Iodo-2-propynyl butylcarbamate was prepared from n-butylamine by reaction with phosgene,2-propargyl-1-alcohol and iodine monochloride.The effects of material ratio,reaction temperature and catalyst on the process were studied.The target product was obtained in overall yield of 93%(99%).