Zhang Xu-De
2012
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Journal
Fine Chemical Intermediates
Abstract
As a key intermediate for the preparation of AQC,6-aminoquinoline was synthesized from 4 nitroaniline and glycerol via Skraup reaction and reduction with 80% hydrazine hydrate catalyzed by 10 % Pd / C.The yield and purity of the target compound was 53% and 99%(HPLC),respectively.The structure of the product was characterized by 1H NMR and ESI-MS.