Li Wei
2011
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Journal
Guangzhou Chemical Industry
Abstract
6-bromoquinoline was synthesized from 4-bromoaniline,glycerol,nitrobenzene by Skraup reaction.The structure of the title compound was characterized by 1HNMR.The effect of the oxidant,reaction time and the adjustment of the pH were discussed.The results showed that the highest yield approached 54% when the oxidant was nitrobenzene,refluxing time was 8 h and pH was 5~6.