Shen Yanhong
2007
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Journal
Journal of Anyang Institute of Technology
Abstract
A method for synthesizing 3,4-dimethoxybenzenamine was reported in this paper.The startingmaterial 3,4-dimethoxybenzene was nitrated by HNO3 under the reaction temperature 0-5℃ to obtain 3,4-dimethoxynitrobenzene,which was reduced by Fe/HAc in mixed solvent to give the title compound,yield:91.4%,purity(HPLC):≥98.0%.