C. Nhu
2013
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Journal
Guangdong Chemical Industry
Abstract
The Arbuzov reaction was carried out with ethyl chloroacetate and triethyl phosphate to obtain the intermediate ethyl 2-(diethoxyphosphoryl)acetate,which then was reacted with 2-bromopropane to obtain the target compound ethyl 2-(diethoxyphosphoryl)-3-methylbutanoate. The overall yield was 79.1 %.