Zheng Chun
2000
Citations
0
Influential Citations
0
Citations
Journal
Journal of Huaihai Institute of Technology
Abstract
N,N diethylaniline is synthesized with benzyl triethylammounium chloride as the phase transfer catalyst.Through orthogonal experiments the optimum process conditions of the reaction are obtained:aniline of 20 mL reacts on bromoethane of 41 mL at 60℃ for 4 hours,with the existence of 40% NaOH solution of 70 mL and benzyl triethylammounium chloride of 1.0 g.The yield of N,N diethylaniline is as high as 76.8% at such process conditions.