Zhao Li-fang
2002
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Journal
Henan Chemical Industry
Abstract
Using methanesulfonyl chloride as raw materials,the methylsulfonamide is synthesized by ammonification.The reaction conditions are discussed.The experimental results show that using cyclohexane as solvent and ethanol as extraction agent,the volume ratio of raw material to solvent is 1∶5,the reaction temperature is 35~40℃,the yield of product reaches 87%~89%.