Wen Zi-qiang
2007
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Journal
Applied Chemical Industry
Abstract
2-Chloro-4-aminophenol was synthesized from 3,4-dichloronitrobenzene by high pressure hydrolysis and reduction reaction,afterwards the addition reaction with perfluoro-vinyl-perfluoro-methyl ether was conducted to synthesize 3-chloro-4-[1,1,2-trifluoro-2-(trifluoromethoxy)-ethoxy]aniline.The overall yield was 72.0%,the product structure was characterized by elemental analyses,IR spectra and 1H NMR,it has characteristics of ready availability of reactant,high yield,good quality,little pollution to environment.