Zhang Ge
2005
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Journal
Fine Chemical Intermediates
Abstract
1, 4-benzenedicarbonyl diisothiocyanate was synthesized by the reaction of 1 , 4-benzenedicarbonyl dichloride with sodium thiocyanate under solid-liquid transfer catalysis. Under the optimal reaction condition, the yield of the reaction was 98.0%, and the purity of the product was 98.2%. The chemical structure of the product was confirmed by IR.