Zhang Shufen
2011
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Journal
Fine chemicals
Abstract
In this study,cationic etherifying agent 2,4-bis(dimethylamino)-6-chloro-[1,3,5]-triazine (BDAT) was synthesized by ultrasonic-assisted method,with cyanuric chloride and dimethylamine as raw materials.It was found out that heterogeneous solid-liquid reaction can proceed smoothly in aqueous solution in ultrasonic-assisted synthesis.The effect of reaction conditions,including ultrasonic time,temperature,pH,ratio of the reactants and ultrasonic irradiation power,on the yield of BDAT was studied.The yield of the target product reached 94% under the optimum conditions.The structure of the product was confirmed by IR,1HNMR and MS spectroscopy.