G. David, D. Morris, E. L. Short
Apr 1, 1981
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Journal
Journal of Labelled Compounds and Radiopharmaceuticals
Abstract
Synthesis of n-heptane labelled with carbon-14 in the 1-position is described. The precedure involves five steps starting with reaction of [14C]carbon dioxide with n-hexyl magnesium bromide and finishing with reduction of [1-14C]n-heptyl bromide. The purity of the final product was more than 97% and the overall yield was 36%.