Zhou Zhi-ming
2010
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Journal
Chinese Journal of Synthetic Chemistry
Abstract
1-(3,3-Dimethyl-2,4-dioxolaneyl-methyl)-4-aryl-1,2,3-triazole(5) was synthesized by 1,3-dipolar cycloaddition of 3,3-dimethyl-2,4-dioxolaneyl-methyl azide and terminal alkyne under ultrasound irradiation for 20 min.The hydroxyl protection of 5 was removed in acidic solution to obtain 1-(2,3-dihydroxylpropyl)-4-aryl-1,2,3-triazole.The structures were characterized by 1H NMR,13C NMR,MS and elemental analysis.