Shen Liqun
2011
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Journal
Chemical Reagents
Abstract
Synthesis of 1-benzyloxy-but-3-en-2-one was reported.It was synthesized by nucleophilic substitution,deprotection,Grignard reaction andoxidation from 2-chloro-1,1-dimethoxy ethane in overall yield of 50.4%.The target product was confirmed by 1HNMR,13CNMR and HRMS.