Zhangjie Shi
2006
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Journal
Chinese Journal of Pharmaceuticals
Abstract
1-Methoxycyclohexene was prepared from cyclohexanone by reaction with dimethyl orthoformate to give 1,1-dimethoxycyclohexane, which subjected to cleavage using BPO4 as catalyst in a fixed bed at 240℃under reduced pressure with an overall yield of 83 %.