Zhang Lin-han
2010
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Journal
Chemistry & Bioengineering
Abstract
2-Biphenyl-4-yl-1-morpholin-4-ethanethione was synthesized with morpholine,sulfur and 1-biphenyl-4-yl-ethanone as starting materials under microwave irradiation.By the orthogonal experiment,the optimum reaction conditions were obtained as follows:microwave irradiation power of 950 W,microwave irradiation time of 7 min,the molar ratio(1-biphenyl-4-yl-ethanone∶sulfur∶morpholine)of 1.0∶3.5∶1.5.Under above optimum conditions,the yield of 2-biphenyl-4-yl-1-morpholin-4-ethanethione was 66.20%.