Tu Wei-jun
2013
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Journal
Chemistry and Adhesion
Abstract
The intermediate 2-hydroxy-4,5,6-trimethoxyacetophenone was synthesized via 5-step reactions which were oxidation,reduction,Friedel-Crafts acylation,hydrolysis and methylation with using trimethoxybenzene as raw material.And each step was optimized by the single factor test and the yield was 48%.The structure of the intermediates and the desired compounds were confirmed by IR and 1H-NMR.