Lin Yuan-bin
2007
Citations
0
Influential Citations
0
Citations
Journal
Chemical Intermediates
Abstract
A new route to produce 3,4-dimethoxy phenethylamine was provided.1,2-Dihydroxy benzene was reacted with dimethyl sulfate to get 1,2-dimethoxy benzene,the yield was 96.7%.After the ether was brominated with high-selective bromating agent,the product could be obtained through Grignard reaction,esterification(the yield was 97.0%) and Gabriel reaction(the yield was 68.5%).The conditions were optimized and it provided an effective approach to produce correlative products.