Liu Guang-ming
2010
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Journal
Journal of Dali University
Abstract
Objective: 3-chloro-(4-benzyloxy)-3-benzene propylene aldehyde was synthesized from phenol and acetic anhydride by esterification,Fries rearrangement and Vislsmeier reaction.Methods: Basing on relative literatures,a method of synthesizing 3-chloro-(4-benzyloxy)-3-benzene propylene aldehyde was established and its purity was measured.Results: 3-chloro-(4-benzyloxy)-3-benzene propylene aldehyde was synthesized successfully.Conclusion: The yield of this new chemical was 76.9%,and its melting point 88-90 ℃ and purity was 98.21%.