Li Cheng-fan
2001
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Journal
Journal of Yanbian University
Abstract
Methyl 3-hydroxy-2,2-dimethylpropionate was synthesized by direct conversion of 3-hydroxy-2,2-dimethylpropionaldehyde prepared by aldol condensation of isobuthylaldehyde and formaldehyde,to the methyl ester using chlorine and sodium hydroxide in methanol. And optimum reaction conditions, such as the amount of chlorine and sodium hydroxide, reaction temperature were established.