Li-Na Fu
2003
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Journal
Chemical Reaction Engineering and Technology
Abstract
3methoxy1propanol was synthesized from 3chloro1propanol. The optimum conditions of methoxy substitution reaction were determined as that the mole ratio of sodium methylate to 3chloro1propanol is 1.4~18, the mass content of sodium methylate in methanol solution is 27%~30%, 3chloro1propanol drops off 1h at reaction temperature of 70℃, and the reaction time is 5h. The yield was over 85% which is better than that reported in literatuies.