Zhang Wei
2008
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Journal
Chemistry & Bioengineering
Abstract
Methyl chloroacetate was synthesized from chloroacetic acid and methanol at solvent-free condition under microwave irradiation at 250 W for 10 min,and the yield was up to 91.0%.Then,using BF4 as solvent,3-(methyloxycarbonyl) tegafur was synthesized from tegafur and methyl chloroacetate under microwave irradiation at 250 W for 18 min,and the yield was up to 82.3%.The compounds were characterized by IR,1HNMR,HRMS.