Han Jing
2011
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Journal
Fine Chemical Intermediates
Abstract
Methylamine was converted to N-methylpentylamine via successive reactions with 4-toluene sulfonyl chloride,pentane bromide and deprotection,followed by reaction with methyl acrylate and hydrolysis to give 3-(N-methyl-N-pentylamino) propanoic acid hydrochloride.The overall yield was 63.93%.The structure of the product was confirmed with MS and 1H NMR.