Lin Yuan-bin
2005
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Journal
Chinese Journal of Synthetic Chemistry
Abstract
3-(Trifluoromethyl)-1,1′-biphenyl was synthesized from 3-trifluoromethylaniline through modified Gomberg condensation using t-BuNO_2 as a diazotization reagent and Cu as a catalyst at 40 ℃ for 5 h. The structure was identified by ~1H NMR, ~(13)C NMR and IR.